GAMMA: Harnessing solid-state thermal cycling to Guide microstructure evolution of Additively Manufactured Metallic Alloys

Agency: European Research Council (ERC)
Instrument: Starting Grant 2020
GrantID: 946959
Institutions: École Polytechnique
PI: Manas V. Upadhyay
Core scientific team: N. Mohanan (Ph.D. student), G. D. Lima-Chaves (Ph.D. student), K. A. Abdesselam (Ph.D. student), S. Gaudez (Post-doc), J. G. Santos Macías (Post-doc), K. Chen (Post-doc)
Dates: March 2021 – February 2026
Funds: 1,499,877 €
Webpage: https://cordis.europa.eu/project/id/946959

Aim: To highlight the important role of solid-state thermal cycling (SSTC) on microstructure evolution during AM, and to show how SSTC can be harnessed to design microstructures with desired mechanical responses.

Objectives:

  • Propose and perform experiments to quantify the microstructural changes brought about solely by SSTC, and to identify the underlying micro-mechanisms.
  • Develop and validate theoretical and fast numerical models to gain deep insight on dynamics of micro-mechanisms and predict polycrystalline evolution due to SSTC.
  • Use the novel models in synergy with experiments to tailor AM process parameters and suggest in-process/post-process thermo-mechanical treatments in order to guide the microstructure evolution in the solid-state and optimize material properties and performance.

Methods:

  • Development of a miniature LMD machine for synchrotron X-ray experiments
  • Designing a novel coupling between a continuous-wave laser and an SEM (CW Laser-SEM) to facilitate microstructure characterization inside an SEM without mechanical polishing by preventing oxidation
  • SEM and TEM characterization using the same capabilities from project MiAM
  • Theoretical development and numerical implementation of novel dislocation and polycrystalline thermomechanical models to study microstructure evolution during thermal cycling.
  • Establishing novel experiment-modelling synergies extended to AM

Expected Impact and Output:

  • Filling a significant knowledge gap in understanding role of thermal cycling on micromechanisms and microstructure evolution occurring during metal AM of steels and Ti-alloys.
  • Proposed novel energy-efficient rapid in-process/post-process laser treatments to alter/fine tune mechanical performance of alloys.
  • Directly inspired follow-on projects, GISTEAM3 (GIS HEAD), LaserSurf (CIEDS) and IMP3D (ANR), and preparation of an ERC Consolidator Grant proposal as well as Proof-of-concept proposal (2026).
  • As of Sep 2025, delivered 19 journal publications, 2 patents, 3 keynote lectures, and 24 invited talks

Publication list:

  1. J. Dumbre, Z. Tong, Y. Chen, A. Rack, N. Isac, M. V. Upadhyay, M. Easton and D. Qiu
    “Impact of build process on microstructural evolution in laser directed energy deposition of Ti-8.5Cu Alloy: An in situ synchrotron X-ray imaging and post-build electron microscopy study”
    Additive Manufacturing, 109 (2025) 104841
    DOI: 10.1016/j.addma.2025.104841 Open Access
  1. K. A. Abdesselam, S. Gaudez, S. van Petegem, V. Honkimäki, S. Hallais, L. Cornet, M. Vallet and M. V. Upadhyay
    “Altering microstructure and enhancing mechanical properties during direct energy deposition of Ti-6Al-4V via in-process laser heat treatments”
    Materials & Design, 254 (2025) 113997
    DOI: 10.1016/j.matdes.2025.113997 Open Access
  1. J. G. Santos Macías, K. Chen, A. Tanguy, M. Vallet, L. Cornet, V. Michel and M. V. Upadhyay
    “High-vacuum laser treatments enhance strength, ductility and fatigue limit of additively manufactured stainless steel”
    Materials & Design, 254 (2025) 114064
    DOI: 10.1016/j.matdes.2025.114064 Open Access
  1. C. B. Larsen, S. Samothrakitis, R. Woracek, E. Polatidis, J. Čapek, M. V. Upadhyay, M. Tovar, S. Schmidt and M. Strobl
    “Exploring Grain-Resolved Strain Tensors and Non-Uniform Lattice Deformations with Laue 3DNDT”
    Acta Materialia, 289 (2025) 120869
    DOI: 10.1016/j.actamat.2025.120869 Open Access
  1. G. D. Lima Chaves, A. Acharya and M. V. Upadhyay
    “A finite deformation theory of dislocation thermomechanics”
    Journal of the Mechanics and Physics of Solids, 200 (2025) 106141
    DOI: 10.1016/j.jmps.2025.106141 Open Access
    Preprint DOI: arXiv.2409.17194 Open Access
  1. S. Gaudez, D. Weisz-Patrault, K. A. Abdesselam, H. Gharbi, V. Honkimäki, S. van Petegem and M. V. Upadhyay
    “Estimating elastic and thermal contributions to lattice strains from operando X-ray diffraction measurements using fast simulations”
    Additive Manufacturing, 101 (2025) 104674
    DOI: 10.1016/j.addma.2025.104674 Open Access
  1. A. F. Chadwick, J. G. Santos Macías, A. Samaei, G. Wagner, M. V. Upadhyay and P. W. Voorhees
    “On microstructure development during laser melting and resolidification: An experimentally validated simulation study”
    Acta Materialia, 282 (2025) 120482
    DOI: 10.1016/j.actamat.2024.120482 Open Access
  1. M. V. Upadhyay, S. Gaudez and W. Pantleon
    “Dislocation structure evolution during metal additive manufacturing”
    IOP Conference Series: Materials Science and Engineering, 44th Risø International Symposium on Materials Science (RISO 2024) 02/09/2024 – 06/09/2024 Roskilde, Denmark, 1310 (2024) 012012
    DOI: 10.1088/1757-899X/1310/1/012012 Open Access
  1. K. Chen, J. G. Santos Macías, N. Isac, M. Vallet, L. Cornet and M. V. Upadhyay
    “Silicon mediated twin formation in laser direct energy deposited 316L stainless steel”
    Scripta Materialia, 253 (2024) 116257
    DOI: 10.1016/j.scriptamat.2024.116257 Open Access
  1. M. V. Upadhyay and J. Viñals
    “Coupling Phase Field Crystal and Field Dislocation Mechanics for a consistent description of dislocation structure and elasticity”
    European Journal of Mechanics-A/Solids, 108 (2024) 105419
    DOI: 10.1016/j.euromechsol.2024.105419 Open Access
  1. N. Mohanan, J. G. Santos Macías, J. Bleyer, T. Helfer, M. V. Upadhyay
    “Intergranular stress and plastic strain formation during laser scanning of additively manufactured stainless steel: An experimentally-driven thermomechanical simulation study”
    Materialia, 34 (2024) 102082
    DOI: 10.1016/j.mtla.2024.102082 Open Access
  1. G. D. Lima-Chaves and M. V. Upadhyay
    “Finite element implementation of the thermal field dislocation mechanics model: study of temperature evolution due to dislocation activity”
    Computer Methods in Applied Mechanics and Engineering, 421 (2024) 116763
    DOI: 10.1016/j.cma.2024.116763 Open Access
  1. S. Gaudez, M. Ben Haj Slama, E. Héripré, L. Yedra, M. Scheel, S. Hallais and M. V. Upadhyay
    “A synchrotron transmission X-ray microscopy study on precipitate evolution during solid-state thermal cycling of a stainless steel”
    Additive Manufacturing, 73 (2023) 103692
    Preprint DOI: 10.2139/ssrn.4379782 Open Access
    DOI: 10.1016/j.addma.2023.103692
  1. S. Gaudez, K. A. Abdesselam, H. Gharbi, Z. Hegedüs, U. Lienert, W. Pantleon and M. V. Upadhyay
    “High resolution reciprocal space mapping reveals dislocation structure evolution during 3D printing”
    Additive Manufacturing, 71 (2023) 103602
    Preprint DOI: 10.2139/ssrn.4367212 Open Access
    DOI: 10.1016/j.addma.2023.103602
  1. S. Gaudez, M. Ben Haj Slama, A. Kaestner and M. V. Upadhyay
    “3D deep convolutional neural network segmentation model for precipitates and porosities identification in synchrotron X-ray tomograms”
    Journal of Synchrotron Radiation, 29 (2022) 1232 – 1240
    DOI: 10.1107/S1600577522006816 Open Access
  1. M. Ben Haj Slama, L. Yedra, E. Héripré and M. V. Upadhyay
    “Insight on precipitate evolution during additive manufacturing of stainless steels via in-situ heating-cooling experiments in a transmission electron microscope”
    Materialia, 21 (2022) 101368
    DOI: 10.1016/j.mtla.2022.101368
    HAL (preprint): hal-03570116 Open Access
  1. Invited Contribution: M. V. Upadhyay and J. Bleyer
    “Dislocation transport using a time-explicit Runge-Kutta discontinuous Galerkin finite element approach”
    Special Issue: “Emerging Leaders 2021
    Modelling and Simulation in Materials Science and Engineering, 30 (2022) 034002
    DOI: 10.1088/1361-651X/ac44a7
    HAL (preprint): hal-03466796 Open Access
  1. Review article: S. Lucarini, M. V. Upadhyay and J. Segurado
    “FFT based approaches in micromechanics: fundamentals, methods and applications”
    Modelling and Simulation in Materials Science and Engineering, 30 (2022) 023002
    DOI: 10.1088/1361-651X/ac34e1 Open Access
  1. M. V. Upadhyay, M. Ben Haj Slama, S. Gaudez, N. Mohanan, L. Yedra, S. Hallais, E. Héripré and A. Tanguy
    “Non-oxide precipitates in additively manufactured austenitic stainless steel”
    Scientific Reports, 11 (2021) 10393
    DOI: 10.1038/s41598-021-89873-2 Open Access